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An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation
Molecules, 19 (2014), 6; 7610-7620. https://doi.org/10.3390/molecules19067610
Gašo-Sokač, Dajana; Bušić, Valentina; Cetina, Mario; Jukić, Marijana

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Gašo Sokač, D., Bušić, V., Cetina, M. i Jukić, M. (2014). An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation. Molecules, 19. (6), 7610-7620. doi: 10.3390/molecules19067610

Gašo Sokač, Dajana, et al. "An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation." Molecules, vol. 19, br. 6, 2014, str. 7610-7620. https://doi.org/10.3390/molecules19067610

Gašo Sokač, Dajana, Valentina Bušić, Mario Cetina i Marijana Jukić. "An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation." Molecules 19, br. 6 (2014): 7610-7620. https://doi.org/10.3390/molecules19067610

Gašo Sokač, D., et al. (2014) 'An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation', Molecules, 19(6), str. 7610-7620. doi: 10.3390/molecules19067610

Gašo Sokač D, Bušić V, Cetina M, Jukić M. An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation. Molecules [Internet]. 2014. [pristupljeno 17.04.2024.];19(6):7610-7620. doi: 10.3390/molecules19067610

D. Gašo Sokač, V. Bušić, M. Cetina i M. Jukić, "An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation", Molecules, vol. 19, br. 6, str. 7610-7620, 2014. [Online]. Dostupno na: https://urn.nsk.hr/urn:nbn:hr:201:329306. [Citirano: 17.04.2024.]

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Naslov (engleski)An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation
AutorDajana Gašo-Sokač
AutorValentina Bušić
AutorMario Cetina
AutorMarijana Jukić
Autorova ustanovaSveučilište u Zagrebu
Tekstilno-tehnološki fakultet
(Zavod za primijenjenu kemiju)
Znanstveno / umjetničko
područje, polje i grana		PRIRODNE ZNANOSTI
Kemija
Sažetak (engleski)
Quaternary salts of pyridoxal oxime have been synthesized by the quaternization of pyridoxal oxime with substituted phenacyl bromides using microwave heating. Microwave-assisted rapid synthesis was done both in solvent (acetone) and under solvent-free conditions. Good to excellent yields (58%94%) were obtained in acetone in very short reaction times (35 min) as well as in the solvent-free procedure (42%78%) in very short reaction times (710 min) too. Effective metodologies for the preparation of pyridoxal oxime quaternary salts, having the advantagies of being eco-friendly, easy to handle, and performed in shorter reactions time are presented. The structure of compound 7, in which a 4-fluorophenacyl moiety is bonded to the pyridinium ring nitrogen atom, was unequivocally confirmed by the single-crystal X-ray diffraction method.
Ključne riječi (engleski)
Jezikengleski
Vrsta publikacijeZnanstveni rad - Izvorni znanstveni rad
Status objaveObjavljen
Vrsta recenzijeRecenziran - međunarodna recenzija
Verzija publikacijeObjavljena verzija rada (izdavačev PDF)
Naslov časopisaMolecules
Brojčani podacivol. 19, br. 6, str. 7610-7620
e-ISSN1420-3049
DOIhttps://doi.org/10.3390/molecules19067610
URN:NBNurn:nbn:hr:201:329306
Datum objave publikacije2014
URL dokumentahttp://www.mdpi.com/1420-3049/19/6/7610/htm
Vrsta resursaTekst
Prava pristupaOtvoreni pristup
Uvjeti korištenjaIkona licence Zaštićeno autorskim pravom.
Datum i vrijeme pohrane2017-02-10 12:55:49