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Scientific paper - Original scientific paper
An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation
Molecules, 19 (2014), 6; 7610-7620. https://doi.org/10.3390/molecules19067610
Gašo-Sokač, Dajana; Bušić, Valentina; Cetina, Mario; Jukić, Marijana

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Gašo Sokač, D., Bušić, V., Cetina, M. & Jukić, M. (2014). An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation. Molecules, 19. (6), 7610-7620. doi: 10.3390/molecules19067610

Gašo Sokač, Dajana, et al. "An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation." Molecules, vol. 19, no. 6, 2014, pp. 7610-7620. https://doi.org/10.3390/molecules19067610

Gašo Sokač, Dajana, Valentina Bušić, Mario Cetina and Marijana Jukić. "An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation." Molecules 19, no. 6 (2014): 7610-7620. https://doi.org/10.3390/molecules19067610

Gašo Sokač, D., et al. (2014) 'An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation', Molecules, 19(6), pp. 7610-7620. doi: 10.3390/molecules19067610

Gašo Sokač D, Bušić V, Cetina M, Jukić M. An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation. Molecules [Internet]. 2014 [cited 2024 December 29];19(6):7610-7620. doi: 10.3390/molecules19067610

D. Gašo Sokač, V. Bušić, M. Cetina and M. Jukić, "An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation", Molecules, vol. 19, no. 6, pp. 7610-7620, 2014. [Online]. Available at: https://urn.nsk.hr/urn:nbn:hr:201:329306. [Accessed: 29 December 2024]

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Metadata
Title (english)An Efficient Synthesis of Pyridoxal Oxime Derivatives under Microwave Irradiation
AuthorDajana Gašo-Sokač
AuthorValentina Bušić
AuthorMario Cetina
AuthorMarijana Jukić
Author's institutionUniversity of Zagreb
Faculty of Textile Technology
(Department of Applied Chemistry)
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract (english)
Quaternary salts of pyridoxal oxime have been synthesized by the quaternization of pyridoxal oxime with substituted phenacyl bromides using microwave heating. Microwave-assisted rapid synthesis was done both in solvent (acetone) and under solvent-free conditions. Good to excellent yields (58%94%) were obtained in acetone in very short reaction times (35 min) as well as in the solvent-free procedure (42%78%) in very short reaction times (710 min) too. Effective metodologies for the preparation of pyridoxal oxime quaternary salts, having the advantagies of being eco-friendly, easy to handle, and performed in shorter reactions time are presented. The structure of compound 7, in which a 4-fluorophenacyl moiety is bonded to the pyridinium ring nitrogen atom, was unequivocally confirmed by the single-crystal X-ray diffraction method.
Keywords (english)
Languageenglish
Publication typeScientific paper - Original scientific paper
Publication statusPublished
Peer reviewPeer review - international
Publication versionPublished version
Journal titleMolecules
Numberingvol. 19, no. 6, pp. 7610-7620
e-ISSN1420-3049
DOIhttps://doi.org/10.3390/molecules19067610
URN:NBNurn:nbn:hr:201:329306
Publication2014
Document URLhttp://www.mdpi.com/1420-3049/19/6/7610/htm
Type of resourceText
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2017-02-10 12:55:49