prikaz prve stranice dokumenta Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone
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Scientific paper - Original scientific paper
Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone
Molecules, 13 (2008), 11; 2786-2795. https://doi.org/10.3390/molecules13112786
Gazivoda, Tatjana; Raić-Malić, Silvana; Hergold-Brundić, Antonija; Cetina, Mario

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Gazivoda, T., Raić Malić, S., Hergold Brundić, A. & Cetina, M. (2008). Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone. Molecules, 13. (11), 2786-2795. doi: 10.3390/molecules13112786

Gazivoda, Tatjana, et al. "Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone." Molecules, vol. 13, no. 11, 2008, pp. 2786-2795. https://doi.org/10.3390/molecules13112786

Gazivoda, Tatjana, Silvana Raić Malić, Antonija Hergold Brundić and Mario Cetina. "Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone." Molecules 13, no. 11 (2008): 2786-2795. https://doi.org/10.3390/molecules13112786

Gazivoda, T., et al. (2008) 'Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone', Molecules, 13(11), pp. 2786-2795. doi: 10.3390/molecules13112786

Gazivoda T, Raić Malić S, Hergold Brundić A, Cetina M. Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone. Molecules [Internet]. 2008 [cited 2024 October 27];13(11):2786-2795. doi: 10.3390/molecules13112786

T. Gazivoda, S. Raić Malić, A. Hergold Brundić and M. Cetina, "Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone", Molecules, vol. 13, no. 11, pp. 2786-2795, 2008. [Online]. Available at: https://urn.nsk.hr/urn:nbn:hr:201:606992. [Accessed: 27 October 2024]

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Title (english)Synthesis and Structural Characterization of the 5-(2- Haloethyl)pyrimidines - Hydrogen-Bonded chains in a-(1- Carbamyliminomethylene)-g-Butyrolactone
AuthorTatjana Gazivoda
AuthorSilvana Raić-Malić
AuthorAntonija Hergold-Brundić
AuthorMario Cetina
Author's institutionUniversity of Zagreb
Faculty of Textile Technology
(Department of Applied Chemistry)
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract (english)
Three novel 5-(2-haloethyl)pyrimidine derivatives were synthesized and characterized by 1H-NMR, 13C-NMR, MS, IR spectra and elemental analysis. Iodine and chlorine atoms in the C-5 side chain were introduced by reaction of 5-(2- hydroxyethyl)pyrimidine with hydroiodic acid and phosphoryl chloride, respectively. The structure of the intermediate a-(1-carbamyliminomethylene)-g-butyrolactone was determined by X-ray crystal structure analysis. The molecule deviates very slightly from planarity. Three NHO hydrogen bonds link the molecules into one-dimensional chains of edge-fused rings.
Keywords (english)
Languageenglish
Publication typeScientific paper - Original scientific paper
Publication statusPublished
Peer reviewPeer review - international
Publication versionPublished version
Journal titleMolecules
Numberingvol. 13, no. 11, pp. 2786-2795
e-ISSN1420-3049
DOIhttps://doi.org/10.3390/molecules13112786
URN:NBNurn:nbn:hr:201:606992
Publication2008
Document URLhttp://www.mdpi.com/1420-3049/13/11/2786/htm
Type of resourceText
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2017-02-10 12:17:04